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An Ideal Restorative Material: Generating Smoothness in Dental Ceramics

Kerem Yilmaz, DDS; and Pelin Ozkan, DDS

February 2012 Issue - Expires February 28th, 2015

Inside Dental Technology

Abstract

Occlusal corrections, acidulated phosphate fluoride applications, carbonated beverages, or air-powder abrasion procedures can roughen the surface of restorations. Once deteriorated, porcelain surfaces need to be repolished. These surfaces can be reglazed or polished through various intraoral and extraoral polishing kits. Although technicians and clinicians often seek studies on the effect of repeated firings on coherence between metal and ceramic, the color of the porcelain, fluorescence, microstructure, and brightness, only a limited number of studies are available in the literature. This article reviews the available literature and presents methods for generating a smooth surface and assessing surface roughness. It also discusses the differences between glazing and mechanical polishing, highlighting the importance of mechanical polishing of dental ceramics.

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Throughout dental history, dentists and technicians have continually searched for the ideal restorative material. Dental ceramics commonly are used to serve this purpose because they are biocompatible and semitransparent in appearance; and they can create esthetic restorations, bear heavy loads, and have a thermal expansion coefficient suitable for dental structure. Currently, studies on porcelain have intensified, especially research on the durability, surface features, and esthetics of this restorative material.1,2

The Importance of a Smooth Surface

The surface of all dental restorative materials should be esthetic and smooth. A smooth surface is important in three terms: function, esthetics, and biologic compatibility. Rough surfaces can decrease the flexural strength of material.3 Opposite hard tissues can be abraded, and consequently, the restored teeth can become worn.4-6 Stain, plaque, and tartar can accumulate.5,7 As a result, the susceptibility to infection in oral soft tissues and caries increases.8,9 Because the free surface energy is lower at uneven surfaces than at smooth ones, microorganisms can easily adhere and colonize.10,11 Further, the esthetic quality of the restoration can decrease.12

With ceramic restorations, the glaze process helps prevent some of these problems. Plaque cannot accumulate on the glazed surface, and the brightness and surface features of the restoration can be retained long term.13 A smooth surface improves the flexural strength of the restoration and decreases abrasion against opposite teeth.14,15

Literature Studies

The literature clearly shows that grinding, polishing, and glazing increase a restoration’s flexural strength. Many studies found that mechanical polishing increases the surface resistance of a ceramic restoration more than the natural glaze and overglaze processes do.16-18 On the contrary, Sherill and O’Brien19 could not find any difference in flexural strength between ceramics that were mechanically polished and those that were glazed; however, Giordano et al14 found that overglazing, grinding, and polishing all significantly increased the flexural strength of ceramic restorations.

Methods to Generate a Smooth Surface

Glaze Process

Before final cementation, a restoration should have a completely smooth surface. This surface can be created only during the final glaze process in the dental laboratory. However, superficial defects can be covered with a surface polisher. The goal is to cycle the restoration through a porcelain furnace at a time and temperature schedule that achieves the proper surface quality, without causing any functional or esthetic damage.20-23

A lower temperature and longer time cycle should be the ceramist’s basic aim. In this way, the pyroplasticity of the crown is controlled to a level at which the surface will assume an enamel-like sheen but will not slump or flow at critical line angles. The ceramist must be aware that as the furnace temperature rises, the viscosity of dental glasses decreases. The ceramist must control this viscosity and use it to his or her advantage.23

A natural-appearing restoration surface can be created with two different glazing methods: overglaze (also called applied glaze) and natural glaze (also called self glaze).22,24 Overglaze is the addition of glass material that is vitrified at a low temperature and decreases the heat of fusion. Natural glaze keeps the surface of material at the temperature of its last firing without adding any other material.25

Overglaze Technique: When external stains need to be applied or a labial margin needs to be created, the porcelain should not be exposed to high temperatures, ruling out a natural glazing. Overglazing should be used to prevent damage to the stains or labial margin. Overglaze is generated by exposing a low temperature porcelain (generally) to a temperature that is 20°C to 60°C below the firing temperature.23,26

Natural Glaze Technique: A natural glaze refers to the process in which the restoration is fired to a temperature that is usually equal to or slightly higher than the original firing temperature. If the crown is to have a natural glaze, it will be fired after the stains are applied, according to the porcelain manufacturer’s instructions. The restoration should be first allowed to dry at the entrance of the furnace muffle until the stain medium has evaporated completely, leaving a dry, chalky surface. Then, the crown is inserted into the furnace slowly and fired to the manufacturer’s recommended glazing temperature for a short period, usually 1 to 2 mins, until the outer surface of the porcelain develops the desired level of gloss. The porcelain surface of the restoration is exposed to temperatures high enough to permit the porcelain to fuse together and create a smooth, glossy outer “skin.” This process is performed at atmosphere pressure. The irregularities and superficial defects on the porcelain surface are closed while the surface melts slightly during firing, creating a smooth and glazed surface.24,27

Mechanical Polishing

Although dental porcelains almost meet the needs expected from a restorative material, they have an important disadvantage. These materials may cause opposite dental structures to be extremely abraded. Most damage happens with contact of uneven surfaces under the occlusive forces. Besides occlusal regulations, acidulated phosphate fluoride applications, carbonated beverages, or air-powder abrasion processes can create unevenness after a restoration is placed. Periodic repair of uneven porcelain surfaces can decrease the abrasion on teeth, reduce the risk of porcelain fracture, and provide the continuity of biologic and esthetic criteria by avoiding accumulation of tartar.28-31

When a porcelain surface loses its luster, it needs to be repolished. It can be either reglazed or polished with various polishing instruments and pastes. The restoration is polished in the patient’s mouth or reglazed in the dental laboratory. When a restoration is reglazed, chairtime for the patient is minimal. However, because reglazing is performed at the dental laboratory, it requires multiple office visits. Ceramic restoration in a furnace at high temperatures may cause destruction because of trapped moisture from the saturation in the oral environment; and therefore, in-laboratory reglazing is typically considered not the best option. After the reglazing procedure, the laboratory technician repolishes the surface extraorally, which allows greater control of the polish.32,33 For this reason, literature studies concentrate on the effects of diamond drills, flexible discs, silicone polishers, and diamond polishing pastes34,35 Although intaroral polishing rarely is performed in the United States, studies have found that the preferred techniques for repolishing are: 1) smoothing the contours with flexible diamond discs, diamond burs, polymer stones, or green stones (silicon carbide); 2) finishing with white stones or rubber discs and conical-shaped rubber tips; and 3) polishing with diamond pastes and felt, conical-shaped or thin rubber discs, or a brush.36,37

Many studies focused on determining the best method of creating a smooth surface on ceramic restorations. A literature review revealed that glazing or mechanical polishing methods are performed to recreate a smooth surface. Generally, stones or diamond drills are used to correct the ceramic before an overglaze or natural glaze is applied. The authors found that most studies on uneven surface texture are oriented toward determining the efficacy or deficiency of mechanical polishing compared with natural glaze or overglaze processes.

Most of these studies used abraders consecutively (diamond bur, rubber disc, diamond paste) or a sequential set of polishers from an available polishing kit. Some studies of the consecutive polishing method used diamond paste in the final phase.12,15,38-40 Other studies used available kits without diamond paste.40-42

Table 1 summarizes the findings of published studies that compared glazing and mechanical polishing. On review, the authors found that the study results depended on which ceramic and polishing method was used. For example, Patterson and colleagues40 declared that if diamond burs are used before a polishing kit, the resulting ceramic surface is smooth but not as smooth as when glaze is applied.

Polishing efficacy also depends on each material’s structure. For example, Sasahara and colleagues31 found that the degree of surface smoothness achieved was based on the leucite content of the porcelain. Further, they noted that to find the appropriate polishing method for each ceramic can be difficult because of varying microstructures. The researchers emphasized that using a ceramic with low leucite content and applying a diamond paste during polishing can increase surface smoothness. To further this point, Al-Wahadni13 found that a high crystal content in a ceramic material can lead to an uneven surface when polished.

Repeated Firings

Although dental porcelains and the preparation techniques have evolved, achieving an esthetic match with the existing dentition can be difficult and require careful planning. Because gold is expensive, there is interest in base metal alloys as the supporting structure of porcelain-fused-to-metal ceramic restorations. Before being placed on the market, these alloys were studied in both laboratory and clinical settings. Besides various compatibility tests (connection, thermal, contour clarity), the studies examined the effect of repeated firings on color, fluorescence, microstructure, and brightness of the fused porcelains.43-47

The solvents were added by manufacturers to decrease the heat of fusion in porcelains. These solvents have a high rate of fluidity, which helps form a glazed surface. However, the thickness of this glaze layer can decrease from repeated firings and intraoral abrasion. The surface is softened, and the glaze layer is removed by repeated firings, decreasing the surface roughness (Figure 1, Figure 2, Figure 3, Figure 4, Figure 5, Figure 6, Figure 7, Figure 8, Figure 9, Figure 10). The mean matrix of porcelain structure, being highly fluid, moves toward the surface of the porcelain and helps form a natural glazed surface. The necessary amount of matrix required to form a natural glazed surface decreases after repeated firings.45

As the number of firings increases, the dimensions of the pores in a porcelain’s structure decrease, creating a vitreous structure. This decrease in the dimensions of the pores causes the porcelain’s rigidity to increase and its flexibility to decrease.52 Repeated firings also cause porcelain’s color pigments to burn and a mass of porcelain to accumulate, creating devitrification. The authors conclude that, based on available data, repeated firings of porcelain restorations should be minimized.45,48

Studies on the effects of repeated firings on surface smoothness are limited. Barghi45 researched the effects of repeated firings on color and glaze and found that after nine firings, a natural glaze layer appears on the surface and the choice of metal alloy did not affect the color or glaze. Mackert and Williams49 researched the effects of repeated firings on the formation of microfractures in the ceramic. They concluded that repeated firings affected the density of microfracture after 1, 3, 7, and 15 firings, but that this finding was not clinically significant. Özkan and Öztaş50 researched the effects of repeated firings on leucite crystals in dental ceramics. They determined that after repeated firings, the porcelain structure and the diffraction pattern of leucite crystals exhibited minimal change, which was not clinically significant. Isgro and colleagures51 researched the effects of repeated firings on thermal distortion in one glass ceramic core, four commercially available veneering porcelains, and two experimental veneering porcelain materials. Measurements on the phase of wash, 1. dentine, 2. dentine, 1. glaze, and 2. glaze were made by using the examples of different veneer ceramics; consequently, the researchers concluded that the thermal expansion coefficient is associated with chemical structure. It was found that when compared with other ceramic compositions, those consisting of glass and aluminum display a more stabile and resistive manner during repeated firings.

Methods to Assess Surface Roughness

Visual assessment, scanning electron microscopy (SEM), profilometry, laser specular reflectance, or atomic force microscopy (AFM) devices can be used for investigating the surface of dental materials.52

Profilometry devices commonly are used for assessing the roughness of a material’s surface. A diamond-scanning probe on the device examines the sample’s surface, and the findings of surface roughness are calculated digitally and recorded.53 Many parameters can be assessed using profilometry devices, with the most common being average roughness deviation (Ra) and root-mean-square (rms) roughness deviation (Rq).54 AFM is used for the studies of abrasion, binding, cleansing, corrosion, acidification, friction, lubrication, and coating. AFM systems use a topographic surface view at the nanometer level to measure the forces between molecules (nN, pN).53,55,56

A review of the literature revealed that usually SEM and profilometry31,34,39,41,42,57 or rarely SEM and visual assessment43 or AFM and profilometry6 are used together. There are also studies that used a single method to analyze the surface smoothness of dental ceramics, for example, SEM,38 visual assessment,12 AFM,58 laser specular reflectance system,45 or profilometry.13,59

Investigating a ceramic’s surface with AFM provides a 3-dimensional (3D) view and allows high-resolution topographic imaging of sample surfaces. Compared with profilometry and visual assessment, AFM provides greater detail. AFM gives the Ra values of the measured samples. Various details can be observed including densely located elevations or valleys; tiny, small, and spiny juts; smooth and flat parts; cracks, breaches, craters, or holes; wide angled and round elevations and valleys; deteriorated surface images; asymmetric or parallel areas; and shiny, smoothness surfaces.6,58,60 Although AFM can be performed directly on the material’s surface (without a coating), its 3D topographic view and numerical parameters of surface smoothness are difficult to repeat because the scanning field is smaller than in other methods.61,62

Conclusion

With today’s ceramic materials, older restorations whose surfaces have roughened can be resmoothed with finishing and polishing products.13 Using various intraoral and extraoral porcelain polishing kits, smoothness levels equal or better than those attained through glazing procedures can be obtained.31

Rough surfaces lead to many problems, including lower flexural strength, abrasion on opposite hard tissues, staining of restoration surfaces, accumulation of plaque and tartar, infection of oral soft tissues, and caries formation. When a porcelain surface loses its luster, it needs to be repolished. It can be either reglazed or polished with various polishing instruments and pastes. Ceramic restoration in a furnace at high temperatures may cause destruction because of trapped moisture from the saturation in the oral environment. For this reason, literature studies concentrate on the effects of diamond drills, flexible discs, silicone polishers, and diamond polishing pastes.

Visual assessment, SEM, profilometry, laser specular reflectance, or AFM devices can be used for investigating the surface of dental materials. Investigating a ceramic’s surface with AFM provides a 3D view and high-resolution topographic imaging of sample surfaces compared with profilometry and visual assessment. AFM gives the value of mean surface roughness, and various details may be observed, including densely located elevations or valleys; tiny, small, and spiny juts; smooth and flat parts; cracks, breaches, craters or holes; wide angled and round elevations and valleys; deteriorated surface images; asymmetric or parallel areas; and shiny, smoothness surfaces.

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About the Authors

Kerem Yilmaz, DDS
Prosthodontist
Department of Prosthodontics, Faculty of Dentistry
University of Ankara
Ankara, Turkey

Pelin Özkan, DDS
Associate Professor
Department of Prosthodontics, Faculty of Dentistry
University of Ankara
Ankara, Turkey

Figure 1  AFM image (256 x 256 pixel, Solver PRO, NT-MDT Co, www.ntmdt.com) of glazed IPS Classic® metal-ceramic (Ivoclar Vivadent, Inc, www.ivoclarvivadent.us) control sample.

Figure 1

Figure 2  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Classic sample after one firing.

Figure 2

Figure 3  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Classic sample after three firings.

Figure 3

Figure 4  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Classic sample after five firings.

Figure 4

Figure 5  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Classic sample after seven firings.

Figure 5

Figure 6  AFM image (256 x 256 pixel, Solver PRO) of glazed IPS Empress® 2 (Ivoclar Vivadent), control sample.

Figure 6

Figure 7  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Empress 2 sample after one firing.

Figure 7

Figure 8  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Empress 2 sample after three firings.

Figure 8

Figure 9  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Empress 2 sample after five firings.

Figure 9

Figure 10  AFM image (256 x 256 pixel, Solver PRO) of the same IPS Empress 2 sample after seven firings.

Figure 10

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SOURCE: Inside Dental Technology | February 2012

Learning Objectives:

  • understand the importance of a smooth surface on restorations.
  • discuss the up-to-date polishing methods for dental ceramics.
  • compare the differences and advantages of mechanical polishing methods with other repolishing methods.